The applicability of utilizing a variety of thermal mass including phase change materials with commonly used building materials is investigated through the use of simulations and physical testing. The thermal performance and occupant comfort potential of a novel solid-solid phase change material, known as Dal HSM, is compared and contrasted to commonly available forms of thermal mass. Detailed experimentation is conducted to successfully integrate Dal HSM with gypsum and concrete. The measurement of physical characteristics such as compressive strength and modulus of rupture is conducted to ensure that the PCM-composite compound retains the structural integrity to be utilized in a typical building. The use of thermal mass in the Toronto Net Zero house was found to contribute to energy savings of 10-15% when different types of thermal mass were used. The comfort level of the indoor occupants was also found to increase. The performance of Dal HSM was found to be comparable to a commercially available PCM known as Micronal in the heating mode. The cooling mode revealed that Dal HSM provided slightly lower energy savings when compared to Micronal due to a lower phase transition temperature and latent heat. The performance of physical test revealed a decrease in the compressive strength as the concentration of Dal HSM was increased in the PCM-gypsum specimens. Tests were also performed to analyze the impact of increasing the PCM concentration on the flexural strength of PCM-gypsum composite.